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    X-ray Structure Determination: A Practical Guide (Hardback) By (author) George Herbert Stout, By (author) Lyle H. Jensen

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    DescriptionClosely follows an actual structural determination. After some introductory material on the nature of x--rays, the diffraction process, and the internal geometry of crystals, the selection and preparation of a crystal are considered. Techniques of measuring raw x--ray data are covered, plus their reduction into a useable form. The second part discusses both traditional and novel methods of solving the "phasea a problem, the principal difficulty in x--ray structure determination. The third part considers how to extract the most information from the data and how to evaluate its reliability. Finally, there is a discussion of sources of error in practice and interpretation.


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  • Full bibliographic data for X-ray Structure Determination

    Title
    X-ray Structure Determination
    Subtitle
    A Practical Guide
    Authors and contributors
    By (author) George Herbert Stout, By (author) Lyle H. Jensen
    Physical properties
    Format: Hardback
    Number of pages: 480
    Width: 160 mm
    Height: 229 mm
    Thickness: 38 mm
    Weight: 908 g
    Language
    English
    ISBN
    ISBN 13: 9780471607113
    ISBN 10: 0471607118
    Classifications

    B&T Book Type: NF
    BIC E4L: SCI
    B&T Modifier: Region of Publication: 01
    Warengruppen-Systematik des deutschen Buchhandels: 16000
    Ingram Subject Code: SE
    Libri: I-SE
    B&T Merchandise Category: SCI
    B&T General Subject: 710
    B&T Modifier: Academic Level: 02
    Nielsen BookScan Product Class 3: S7.5
    LC subject heading:
    DC19: 548.83
    BISAC V2.8: TEC015000
    LC classification: QD945
    BIC subject category V2: PNT
    BISAC V2.8: SCI016000
    LC subject heading:
    B&T Approval Code: A54702050
    DC22: 548.83, 548/.83
    LC classification: QD945 .S8 1989
    Edition
    2, Revised
    Edition statement
    2nd Revised edition
    Illustrations note
    index
    Publisher
    John Wiley and Sons Ltd
    Imprint name
    John Wiley & Sons Inc
    Publication date
    21 June 1989
    Publication City/Country
    New York
    Table of contents
    PRELIMINARY STAGES. X--Rays. Diffraction of X--Rays. Crystals, Symmetry, and Space Groups. Crystals and Their Properties. Geometric Data Collection. Intensity Data Collection. Data Reduction. Theory of Structure Factors and Fourier Syntheses. Calculation of Structure Factors and Fourier Syntheses. THE PHASE PROBLEM. The Phase Problem. Direct Methods. Patterson Methods. Heavy Atom Methods. Search Methods. Completing the Structure. REFINEMENT AND RESULTS. Refinement of Crystal Structures. Random and Systematic Errors. Derived Results. Ambiguities and Uncertainties. Appendices. Index.