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    The Spectrometric Identification of Organic Compounds (Hardback) By (author) Robert M. Silverstein, By (author) Francis X. Webster, By (author) David Kiemle

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    DescriptionOriginally published in 1962, this was the first book to explore teh identification of organic compounds using spectroscopy. It provides a thorough introduction to the three areas of spectrometry most widely used in spectrometric identification: mass spectrometry, infrared spectrometry, and nuclear magnetic resonance spectrometry. A how-to, hands-on teaching manual with considerably expanded NMR coverage--NMR spectra can now be intrepreted in exquisite detail. This book: Uses a problem-solving approach with extensive reference charts and tables. Offers an extensive set of real-data problems offers a challenge to the practicing chemist


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    Title
    The Spectrometric Identification of Organic Compounds
    Authors and contributors
    By (author) Robert M. Silverstein, By (author) Francis X. Webster, By (author) David Kiemle
    Physical properties
    Format: Hardback
    Number of pages: 512
    Width: 224 mm
    Height: 282 mm
    Thickness: 23 mm
    Weight: 1,315 g
    Language
    English
    ISBN
    ISBN 13: 9780471393627
    ISBN 10: 0471393622
    Classifications

    B&T Book Type: NF
    BIC E4L: SCI
    B&T Modifier: Region of Publication: 01
    LC subject heading:
    BIC subject category V2: PNN
    Ingram Subject Code: SE
    Libri: I-SE
    B&T Merchandise Category: SCI
    B&T General Subject: 710
    B&T Modifier: Academic Level: 02
    Nielsen BookScan Product Class 3: S7.5
    B&T Modifier: Text Format: 06
    LC subject heading:
    Warengruppen-Systematik des deutschen Buchhandels: 16500
    LC subject heading: ,
    BISAC V2.8: SCI013010, SCI013050
    LC subject heading:
    BIC subject category V2: PNFS
    DC22: 543.5
    BISAC V2.8: SCI078000
    LC subject heading: ,
    DC22: 543/.5
    LC classification: QD272.S6 S55 2005
    LC subject heading:
    Thema V1.0: PNN, PNFS, PNR
    Edition
    7, Revised
    Edition statement
    7th Revised edition
    Publisher
    John Wiley and Sons Ltd
    Imprint name
    John Wiley & Sons Inc
    Publication date
    11 October 2005
    Publication City/Country
    New York
    Table of contents
    Chapter 1. Mass Spectrometry. 1.1 Introduction. 1.2 Instrumentation. 1.3 Ionization Methods. 1.4 Mass Analyzers. 1.5 Interpretation of El Mass Spectra. 1.6 Mass Spectra of Some Chemical Classes. Chapter 2. Infrared Spectrometry. 2.1 Introduction. 2.2 Theory. 2.3 Instrumentation. 2.4 Sample Handling. 2.5 Interpretations of Spectra. 2.6 Characteristic Group Absorption of Organic Molecules. Chapter 3. Proton Magnetic Resonance Spectrometry. 3.1 Introduction. 3.2 Theory. 3.3 Instrumentation and Sample Handling. 3.4 Chemical Shift. 3.5 Spin Coupling, Multiplets, Spin Systems. 3.6 Protons on Oxygen, Nitrogen, and Sulfur Atoms. Exchangeable Protons. 3.7 Coupling of Protons to Other Important Nuclei ( 19 F, E, 31 P, 29 Si, and 13 C. 3.8 Chemical Shift Equivalence. 3.9 Magnetic Equivalence (Spin-Coupling Equivalence). 3.10 AMX, ABX, and ABC Rigid Systems with Three Coupling Constants. 3.11 Confirmationally Mobile, Open-Chain Systems. Virtual Coupling. 3.12 Chirality. 3.13 Vicinal and Geminal Coupling. 3.14 Low-Range Coupling. 3.15 Selective Spin Decoupling. Double Resonance. 3.16 Nuclear Overhauser Effect, Difference Spectrometry, 1H 1H Proximity Through Space. Chapter 4. Carbon-13 NMR Spectrometry. 4.1 Introduction. 4.2 Theory. 4.3 Interpretation of a Simple 13 C Spectrum: Diethyl Phthalate. 4.4 Quantitative 13 C Analysis. 4.5 Chemical Shift Equivalence. 4.6 DEPT. 4.7 Chemical Classes and Chemical Shifts. Chapter 5. Correlation NMR Spectrometry; 2-D NMR. 5.1 Introduction. 5.2 Theory. 5.3 Correlation Spectrometry. 5.4 Ipsenol: 1 H- 1 H COSY. 5.5 Caryophyllene Oxide. 5.6 13 C- 13 C Correlations: Inadequate. 5.7 Lactose. 5.8 Relayed Coherence Transfer: TOCSY. 5.9 HMQC - TOCSY. 5.10 ROESY. 5.11 VGSE. 5.12 Gradient Field NMR. Chapter 6. NMR Spectrometry of Other Important Spin 1/2 Nuclei. 6.1 Introduction. 6.2 15 N Nuclear Magnetic Resonance. 6.3 19 F Nuclear Magnetic Resonance. 6.4 29 Si Nuclear Magnetic Resonance. 6.5 31 P Nuclear Magnetic Resonance. 6.6 Conclusion. Chapter 7. Solved Problems. 7.1 Introduction. Chapter 8. Assigned Problems. 8.1 Introduction.