Basic One- and Two-Dimensional NMR Spectroscopy

Basic One- and Two-Dimensional NMR Spectroscopy

Paperback

By (author) Horst Friebolin

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  • Publisher: Wiley-VCH Verlag GmbH
  • Format: Paperback | 442 pages
  • Dimensions: 224mm x 279mm x 43mm | 2,495g
  • Publication date: 1 January 2011
  • Publication City/Country: Weinheim
  • ISBN 10: 3527327827
  • ISBN 13: 9783527327829
  • Edition: 5, EnlargedRevised
  • Edition statement: 5th Revised, Enlarged ed.
  • Illustrations note: 146 schwarz-weiße Abbildungen, 49 schwarz-weiße Tabellen
  • Sales rank: 453,312

Product description

This is the fifth edition of the highly successful, classic textbook for bachelor and master courses, with over 20 % new material and the contents completely revised and updated. Using a minimum of mathematics, it explains the underlying theory of this most important spectroscopic technique in a thorough, yet readily understandable way, covering instrumentation and interpretation of the spectra. It presents all students need to know about 1D, 2D-NMR, solid state and dynamic NMR spectroscopy, as well as NMR imaging, all illustrated by examples for maximum clarity. All the sections include sub-chapters that focus on applications taken from organic, macromolecular, polymer and biochemistry. A must for students and lecturers in chemistry, biochemistry, pharmacy, and life sciences, as well as for spectroscopists.

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Author information

Horst Friebolin did his Ph.D. under the supervison of Prof. R. Mecke at the University of Freiburg, Germany, in 1963. Between 1963 and 1979 he worked at the Institute for electronic materials at the Fraunhofer Society and at the Institute for Macromolecular Chemistry at the University of Heidelberg. After two years in industry (BASF, Ludwigshafen, Germany) he finished 1971 his habilitation and joined in 1972 the Institute for Organic Chemistry at the University of Heidelberg, where he was appointed full Professor in 1974. His research fields are the isolation and characterization of natural products as well as enzyme-catalyzed reactions.

Review quote

From reviews of previous editions: "This book is a pleasure to read and if it does not arouse the student's interest, then it is difficult to see what could. It is clearly written and illustrated ... good value and essential reading for anyone wanting to know more about NMR." Chemistry in Britain "Another paperback that I would advise students to buy ... [it] can be recommended for general purchase by all chemists." New Scientist "This book deserves much praise. If only all authors took as much trouble to produce a work of such clarity and relevance... The book forms an excellent bridge between the very simple texts on spectral interpretation and more specialist works with an emphasis on mathematical theory... This book is highly educational and will be of benefit to those who have to teach NMR and to students and scientists in academic and industrial laboratories... this work is right up to date with an inclusion of most widely used modern NMR methods with a style and content that is superb." NMR in Biomedicine

Back cover copy

This fifth Edition of a bestselling undergraduate/graduate textbook in NMR spectroscopy provides all the basic knowledge of the theory, instrumentation, and especially interpretation of the spectra of this frequently used analytical technique. Everything students need to know about 1D, 2D-NMR, solid state and dynamic NMR spectroscopy as well as NMR imaging is presented in this text, illustrated by examples and applications from organic, macromolecular, polymer and biochemistry. This edition features problems and solutions for the reader to check their understanding.From review of previous editions: "This book is a pleasure to read and if it does not arouse the student's interest, then it is difficult to see what could. It is clearly written and illustrated ...good value and essential reading for anyone wanting to know more about NMR." - Chemistry in Britain"Another paperback that I would advice students to buy ... [it] can be recommended for general purchase by all chemists." - New Scientist"This book deserves much praise. If only all authors took as much trouble to produce a work of such clarity and reliance... The book form an excellent bridge between the very simple texts on spectral interpretation and more specialist works with an emphasis on mathematical theory... This book is highly educational and will be of benefit to those who have to teach NMR and to students and scientists in academic and industrial laboratories... this work is right up to date with an inclusion of most widely used modern NMR methods with a style and content that is superb. " - NMR in Biomedicine..". with it's fourth edition, Friebolin's NMR textbook remains the valuable companion and helpful guide as which it is well-known and appreciated among chemists and other scientists who seek a practical, comprehensive, but easy-to-read introduction into high resolution NMR spectroscopy on organic molecules." - Dr. Ingo Schnell, Max-Planck-Institute for Polymer Research, Mainz, ChemPhysChem

Table of contents

The Physical Basis of NMR Spectroscopy The Chemical Shift Indirect Spin-Spin Coupling Spectrum Analysis and Calculations Double Resonance Experiments Assignment of 1H and 13C Signals Relaxation One-Dimensional NMR Experiments using Complex Pulse Sequences Two-Dimensional NMR Spectroscopy The Nuclear Overhauser Effect Dynamic NMR Spectroscopy (DNMR) Shift Reagents Macromolecules NMR Spectroscopy in Biochemistry and Medicine